SEPARATION AND INFRARED (FT-IR) CHARACTERIZATION OF AROMATIC HYDROCARBONS FROM HIGH BOILING FRACTIONS (>200 oC) OF NIGERIA CRUDE OIL (USING TRICHLOROETHYLENE AS THE ELUANT)

NJOKUNWOGBU, A.N and AMARACHUKWU, OKOYEAGU and ENE, FELICITAS C and IYIOKU, MAGNUS U and ENYI, CATHERINE N (2022) SEPARATION AND INFRARED (FT-IR) CHARACTERIZATION OF AROMATIC HYDROCARBONS FROM HIGH BOILING FRACTIONS (>200 oC) OF NIGERIA CRUDE OIL (USING TRICHLOROETHYLENE AS THE ELUANT). International Research Journal of Applied Sciences, Engineering and Technology, 8 (8). pp. 1-9. ISSN 1573-1405

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Abstract

The separation and characterization of aromatic hydrocarbons from high boiling fractions (>200°C) of Nigeria crude oil is reported. The crude oil was distilled under atmospheric pressure in a glass system, with the help of a paraffin bath. The bottom fraction of the crude oil was fractionated using solvent deasphaltening (in which case n-heptane was used followed by filtration), and elution - adsorption chromatography. The saturates were eluted with n-heptane by liquid chromatography on silica gel while the aromatics were eluted with trichlorethylene. The l.R. analysis of the aromatic extracts showed absorption peaks at 3082.94 cm-1, 3037.06cm-1, 1584.82cm-1, l557.09cm-1, l497.43cm-1, 1247.97cm-1, 931.79cm-1, 907.36cm-1, 841 .53cm-1, 676.46cm-1 and 629.49cm-1 respectively. These absorption peaks are due to the presence of aromatics hydrocarbons

Item Type:	Article
Subjects:	Q Science > Q Science (General)
Divisions:	Faculty of Natural and Applied Sciences
Depositing User:	mrs chioma hannah
Date Deposited:	19 May 2023 14:34
Last Modified:	19 May 2023 14:34
URI:	http://eprints.gouni.edu.ng/id/eprint/4014

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